The difficulty in preparing these materials arises from the fact that these materials have oxide inclusions in the microstructure. Proper specimen preparation retains these oxides and thus eliminates scratching and smearing from these particles. If the specimen is not prepared properly, the microstructure will not be accurately represented.
SECTIONING
MAXCUT Abrasive blade (Cat. No. MAX-C or MAX-I series)
MOUNTING
Compression Mounting with Phenolic, Epoxy or Diallyl Phthalate compression mounting resins
POLISHING
Abrasive/surface |
Lubricant |
Force/ sample |
Speed |
Time |
P220 grit ALO paper |
Water |
5-10 lbs |
100/100 rpm |
Until plane |
1 um DIAMAT diamond on ATLANTIS polishing pad |
DIALUBE Purple Extender |
5-10 lbs |
100/100 rpm |
2 minutes |
0.05 um Nanometer alumina on NAPPAD polishing pad |
|
5-10 lbs |
100/100 rpm |
1 minute |
 |
Aluminum-Silicon Alloy, Polarized 400x |
 |
Aluminum-Silicon Alloy, B.F. 200X |