Cordierite Ceramic
Specimen Preparation (Class 10 Procedures)
The preparation of hard/brittle/porous ceramic materials is not especially difficult with a few simple preparation tricks. First, to minimize grain pull-out which may be falsely characterized as porosity sectioning damage must be minimized. This is accomplished by sectioning with the appropriate diamond wafering blade and using the finest practical abrasive for initial grinding. Planar grinding is best achieved with the use of as small a diamond abrasive as possible on a metal mesh cloth. Note there is a trade-off between planar grinding time (abrasive size) and induced damage. In some cases for ceramics, it is better to take more time and minimize damage at planar grinding in order to reduce overall polishing times. The use of SIAMAT colloidal silica also provides a chemical mechanical polishing (CMP) action which is the most effective means for eliminating both surface and subsurface damage. The combination of SIAMAT colloidal silica with DIAMAT polycrystalline diamond also produces the required surfaces finishes.
SECTIONING
Diamond Wafering blade - medium grit / low concentration
MOUNTING
Castable Mounting with Epoxy or Acrylic resins.
POLISHING
Abrasive/surface |
Lubricant |
Force/ sample |
Speed
(Head/base) |
Time |
Individual
Force mode |
Central Force
mode |
70 micron diamond grinding disk*
|
Water |
5-10 lbs |
200/200 rpm |
Planar
|
|
|
30 um DIAMAT diamond
suspension on CERMESH
Metal
Mesh cloth |
|
5-10 lbs |
200/200 rpm |
5 min |
|
|
6 um DIAMAT diamond
on TEXPAN polishing pad |
SIAMAT
colloidal
silica |
10 lbs |
200/200 rpm |
5 min |
|
|
1 um DIAMAT diamond
on GOLDPAD or ATLANTIS
polishing pad |
SIAMAT
colloidal
silica |
10 lbs |
200/200 rpm |
5 min |
|
|
SIAMAT Colloidal silca
on TEXPAN polishing pad |
|
10 lbs |
200/200 rpm |
5 min |
|
|
*Required for central polishing force. Click here for more information on central vs. individual polishing force polishing.
|
Cordierite Ceramic, 200X, as polished
|
|
Cordierite Ceramic, 200X,
Sputter coated to increase contrast
|
CAUTION:Safety is very important when etching. Be sure to wear the appropriate protective clothing and observe all WARNINGS on chemical manufacuters SDS (Safety Data Sheets). Also review the COMMENTS and CONDITIONS Section for each etchant.
PACE TECHNOLOGIES CONTACT
PACE Technologies
3601 E. 34th St.
Tucson, Arizona 85713
+1-520-882-6598
FAX +1-520-882-6599
email: pace@metallographic.com
https://www.metallographic.com
Information Requests
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PACE TECHNOLOGIES® -
3601 E. 34th St., Tucson, AZ 85713,
USA
Telephone +1-520-882-6598 FAX +1-520-882-6599
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