CLASS 5 Material Preparation Guide

Class 5: Medium Hard, Ductile Metals

Class 5 includes steels and stainless steels with less than 2% carbon. These widely used ferrous alloys vary in microstructure and hardness depending on carbon content and thermal treatment. Metallographic preparation is generally routine, but structure-specific etching and polishing may be required to reveal features like pearlite, ferrite, and martensite.

Hardness Range
150–400 HV (varies with treatment)
Typical Materials
Stainless Steels, Low & Medium Carbon Steels
Preparation Challenge
Minimal; Etch Sensitivity

Material Categories

Low Carbon Steels

Common Types
  • Mild Steel
  • Annealed Steels
  • Structural Steel
Key Features
  • Ferrite + Pearlite microstructure
  • Soft and ductile
  • Low wear resistance

Medium Carbon Steels

Common Grades
  • 1045 Steel
  • 4140 Alloy Steel
  • Tempered Martensite
Key Features
  • Higher strength and hardness
  • Martensite, Bainite, or Pearlite phases
  • Heat treatable

Stainless Steels

Common Types
  • 304 Austenitic
  • 410 Martensitic
  • 316L Low Carbon
Preparation Notes
  • Non-magnetic austenite in 300-series
  • Careful etching to avoid overattack
  • Often shows strain-induced features

Preparation Guide

Key Preparation Challenges

Etch Sensitivity

Overetching can obscure pearlite or martensite; underetching may fail to reveal boundaries.

Surface Relief

Harder phases like martensite may polish unevenly compared to surrounding ferrite.

Strain Artifacts

Cold work or grinding stress may introduce artifacts unless properly relieved.

Smearing

Soft phases like ferrite may smear slightly if force is excessive during polishing.

Recommended Preparation Steps

Sectioning

Standard abrasive cutting is sufficient. Use coolant to avoid heat-induced microstructural changes.

Mounting

Compression mounting is commonly used. Ensure alignment to preserve grain orientation if needed.

Grinding

Start with SiC papers, progressing to finer grits. Minimal pressure reduces deformation in soft areas.

Polishing

Use diamond suspension on a medium-nap cloth. Final polish with colloidal silica for clear grain structure.

Quality Verification

Grain boundaries and phases are clearly visible

No overetched or underetched zones

Minimal polishing relief across phases

No surface strain or cold work artifacts