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4% Picral

General Purpose

Composition

4% Picric Acid in Ethanol

4%

Method

Immersion

Time

10s

Alternative Names

Picric AcidPicral 4%

Tags

carbon-steelcast-ironpearlite

Reveals

Pearlite, cementite, grain boundaries

Typical Results

Excellent for revealing pearlite structure. Does not attack ferrite grain boundaries as strongly as Nital.

Color Effects

Pearlite darkens, ferrite remains light

Compatible Materials

carbon-steelcast-ironpearlitic-steel

Incompatible Materials

stainless-steelmartensitic-steel

Application Method

Method:immersion
Typical Time:10 seconds

Preparation Notes

Mix 4 g picric acid with 100 ml ethanol. Warm slightly to dissolve. CAUTION: Picric acid is explosive when dry.

Application Notes

Immerse sample for 10-20 seconds. Swab if needed. Rinse with ethanol then water.

Troubleshooting

Keep picric acid wet at all times. Never allow to dry. Store in water-wet condition.

Storage Notes

Store in dark bottle, keep wet. Add water if solution dries. Extremely hazardous when dry.

Alternative Etchants

  • 2% Nital
  • 3% Nital

Similar Etchants

  • 2% Nital

ASTM References

ASTM E407