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Modified Kroll's Reagent

Material Specific

Composition

1ml HF, 3ml HNO₃, 100ml H₂O

1%

Method

Swabbing

Time

5s

Alternative Names

Modified Kroll'sKroll's Modified

Tags

titaniumtitanium-alloy

Reveals

Alpha-beta phases, grain boundaries

Typical Results

Less aggressive version of Kroll's reagent. Good for sensitive titanium microstructures.

Color Effects

Alpha phase light, beta phase dark

Compatible Materials

titaniumtitanium-alloy

Incompatible Materials

steelaluminum

Application Method

Method:swabbing
Typical Time:5 seconds

Preparation Notes

CAUTION: HF is extremely hazardous. Mix 1ml HF, 3ml HNO₃, and 100ml water in plastic container. Use fume hood and proper PPE.

Application Notes

Swab sample for 5-15 seconds. Do not immerse. Rinse immediately with copious water.

Troubleshooting

HF causes severe burns. Always use in fume hood with proper PPE. Have calcium gluconate gel available. Less aggressive than standard Kroll's.

Storage Notes

Store in plastic container. Label clearly. Extremely hazardous - follow safety protocols.

Alternative Etchants

  • Kroll's Reagent
  • Ti-AP-16

Similar Etchants

  • Kroll's Reagent

ASTM References

ASTM E407