CLASS 1 Material Preparation Guide

Class 1: Soft, Ductile Materials

Class 1 materials are characterized by their low hardness (typically below 150 HV) and high ductility. These materials present unique challenges in metallographic preparation due to their tendency to deform, smear, and embed abrasive particles. Proper preparation is crucial for revealing true microstructural features and preventing artifacts.

Hardness Range
Below 150 HV
Typical Materials
Aluminum, Copper, Lead, Tin, Zinc
Preparation Challenge
Preventing Deformation

Material Categories

Aluminum Alloys

Common Alloys
  • 2xxx Series (Al-Cu)
  • 6xxx Series (Al-Mg-Si)
  • 7xxx Series (Al-Zn-Mg)
Key Features
  • Age-hardening characteristics
  • Precipitate distribution
  • Grain structure analysis

Copper Alloys

Common Alloys
  • Brass (Cu-Zn)
  • Bronze (Cu-Sn)
  • Beryllium Copper
Key Features
  • Phase distribution
  • Grain size analysis
  • Precipitate morphology

Lead, Tin, Zinc

Material Characteristics
  • Extremely soft (HV < 50)
  • High thermal sensitivity
  • Complex phase structures
Preparation Focus
  • Minimal force application
  • Temperature control
  • Phase preservation

Polymer Matrix Composites

Composite Types
  • Carbon fiber reinforced
  • Glass fiber reinforced
  • Metal matrix composites
Key Considerations
  • Fiber orientation
  • Interface integrity
  • Matrix-fiber bonding

Preparation Guide

Key Preparation Challenges

Deformation

Soft materials are prone to mechanical deformation during cutting and grinding, leading to distorted microstructures.

Smearing

Surface smearing can obscure grain boundaries and second-phase particles.

Abrasive Embedding

Abrasive particles can become embedded in the soft surface, requiring careful cleaning between steps.

Oxide Preservation

Special care is needed to preserve oxide inclusions and prevent their removal during preparation.

Recommended Preparation Steps

Sectioning

Use low-speed abrasive cutting with minimal force. Consider using a coolant to prevent heat generation and subsequent deformation.

Mounting

Compression mounting is preferred for most applications. Use low-pressure mounting for extremely soft materials to prevent deformation.

Grinding

Begin with coarse SiC paper (180-240 grit) and progress through finer grits. Use minimal force and frequent cleaning between steps.

Polishing

Use diamond suspensions on appropriate polishing cloths. Final polish with colloidal silica or alumina to remove any remaining deformation.

Quality Verification

Check for absence of deformation under polarized light

Verify grain boundaries are clearly visible

Ensure second-phase particles are not smeared

Confirm oxide inclusions are preserved