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PACE Technologies Metallographic Preparation CLASS Chart icon

Superalloys with Ceramic Coating
Specimen Preparation (Class 7 Procedures)
Metallographic Class 7 sample preparation

To improve both the wear and temperature resistance of Superalloys, coating of zirconia or other ceramics are applied to the turbine blade. Metallographic analysis is used to determine the quality and integrity of the coating, as well as, any delamination problems. In order to get an accurate measurement on the coating, specimen preparation must focus on minimizing damage to the coating. Minimizing damage as early as the abrasive cutting operation ensures successful preparation. For cutting ceramic coated Superalloys, the MAX-H series blade is recommended. Mounting with a fine EPOCOMP epoxy helps to better protect the surface during grinding and polishing.

Grinding must also minimize damage to the coating, so initial grinding should be with the finest SiC paper which provides acceptable grinding rates (e.g. 320 grit SiC paper). Final grinding down to 1200 grit SiC paper is recommended. For rough polish on a 3 micron diamond on a GOLDPAD polishing cloth produces a moderate finish that is flat across the various materials. For the final polish the use of our newly developed ATLANTIS polishing pad, which is a woven pad on a compressible foam backing produces excellent flatness and surface finishes. This pad, works extremely well for polishing materials of significantly different hardenss (i.e. metal substrate with ceramic coating). To also aid in the polishing of ceramic and metal combination materials, the use of colloidal silica as a lubricant / abrasive produces a chemical mechanical polishing effect (CMP) which provides the best finish and flatness for ceramic coating and metal interfaces.

SECTIONING
MAXCUT Abrasive blade (Cat. No. MAX-E or MAX-I series) (if required)

MOUNTING
Compression Mounting fine EPOCOMP Epoxy compression mounting resins

POLISHING
Abrasive/surface Lubricant Force/ sample Speed
(Head/base)
Time Individual
Force mode
Central Force
mode
240 grit SiC paper*
Water
5-10 lbs 200/200 rpm Planar
  Metallographic central polishing force
320 grit SiC paper
400 grit SiC paper
600 grit SiC paper
800 grit SiC paper
1200 grit SiC paper
Water
5-10 lbs 200/200 rpm 1 min
1 min
1 min
1 min
1 min
Metallographic individual polishing force Metallographic central polishing force
3 um DIAMAT diamond
on GOLDPAD
DIALUBE Purple
Extender
5 lbs 200/200 rpm 2 min Metallographic individual polishing force Metallographic central polishing force
1 um DIAMAT diamond on
ATLANTIS polishing pad
SIAMAT Colloidal
Silica
10 lbs 200/200 rpm 2 min Metallographic individual polishing force Metallographic central polishing force

*Required for central polishing force. Click here for more information on central vs. individual polishing force polishing.

Metallographic micrograph of NiCr plasma spray coating
Zirconia thermal spray coating, as polished Mag 1000x (B.F.)

ETCHING

Common Etchants
PACE Technologies Recommended Etchants

PACE Technologies Etchant Database

CAUTION:Safety is very important when etching. Be sure to wear the appropriate protective clothing and observe all WARNINGS on chemical manufacuters SDS (Safety Data Sheets). Also review the COMMENTS and CONDITIONS Section for each etchant.


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